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Ib hom kev npaj ntawm tsib-leaved chaste ntoo volatile roj

Technical field
Qhov kev tsim kho tam sim no muaj feem xyuam rau tsib-leaved chaste tree volatile oil field, yog ib hom kev npaj ntawm tsib-leaved chaste tree volatile roj.
Cov cuab yeej siv tom qab
Hauv kev lag luam khoom noj khoom haus, sanitas yog ib qho tseem ceeb tshaj plaws additive.Nws yog ib chav kawm yuav tsum tau noj cov khoom noj khoom haus additive uas tiv thaiv cov zaub mov muaj nqis thiab thawj tus cwj pwm yog khoom.Tam sim no cov pa sanitas yog nyob rau hauv feem ntau nrog chemosynthesis sanitas nyob rau hauv lub ntiaj teb no, tab sis luring. chemosynthesis sanitas yog carcinous, teratogenecity thiab cov teeb meem xws li cov zaub mov tsis muaj tshuaj lom uas yooj yim ua rau muaj kev txhawj xeeb ntawm kev sib raug zoo.Nyob rau hauv xyoo tas los no, nrog rau kev loj hlob ntawm tib neeg lub neej thiab theem ntawm kev noj, qhov kev thov ntawm cov zaub mov ua tiav kuj ntau thiab ntau dua. Cov kev hloov pauv rau cov lus qhia xws li "ntsuab" thiab "natural" .Yog li ntawd, kev tshawb fawb thiab kev loj hlob ntawm cov khoom noj muaj txiaj ntsig zoo ntawm cov khoom noj sanitas tsuas yog zoo li ntau dua thiab tseem ceeb dua.Antiseptics rau cov zaub mov ntuj tuaj yeem muab faib ua microbialpreservatives (N, O-Diacetylmuramidase, nisin, tennecetin, epsilon-polylysine), creatural preservative (protamine, propolis, chitosan) thiab cov nroj tsuag qhov chaw tshuaj tua kab mob (tea-polyphenol, cov nroj tsuag tseem ceeb roj, qejin, anthraquinone tshuaj ntsuab). raug cov zaub mov peculiar tsis hnov ​​tsw, muab tshuaj tsw qab, pleev xim rau, anti-oxidant, tshuaj tua kab mob (anticorrosion) thiab lub physiological thiab pharmacological nyhuv nyob rau hauv tas li ntawd, muaj.As ib qho tseem ceeb qhov chaw ntawm natural antiseptic neeg sawv cev, los ntawm cov nroj tsuag tseem ceeb roj, lim tawm npaum, economic, muaj kev nyab xeeb cov khoom noj khoom haus preservatives, muaj kev siv dav dav thiab kev tshawb fawb tseem ceeb heev.
Tam sim no, kev tshawb fawb tshuaj tua kab mob rau cov nroj tsuag yog ntau, raws li nws cov txiaj ntsig kev tshawb fawb, kwv yees tuaj yeem muab faib ua peb hom hauv qab no: ua rau kev tshawb fawb txog kev txwv cov kab mob pathogenic ntawm cov zaub mov spoilage pom cov khoom noj khoom noj khoom haus, txwv kev tshawb fawb ntawm phytopathogen yog. tsim niaj hnub thiab txwv cov nyhuv kev tshawb fawb ntawm tib neeg lub cev pathogenic cov kab mob yog tsim rau cov tshuaj tshiab.Meanwhile, raws li tau muab faib ua dua qhov chaw ntawm kev txiav txim ntawm cov nroj tsuag kev tshawb fawb: extract nroj tsuag tseem ceeb roj thiab nqa tawm antibacterial kev tshawb fawb, keeb kwm ntawm cov nroj tsuag, qia, nplooj. yog nqa tawm mus rau kev sim tshuaj tua kab mob thiab kev tshawb fawb los tiv thaiv kab mob microbial los cog endogenesis fungus extract nrog organic hnyav extraction.
Nyob rau hauv lub hauv paus uas tam sim no invention yog npaj rau tsib-leaved chaste ntoo volatile roj rau extract; yuav siv tau rau lotus rhizome anti-corrosive tshiab-ua; cov cuab yeej biocidal, kev ruaj ntseg raws li cov khoom noj khoom haus cog qoob loo; kom tau txais ntsuab, muaj kev nyab xeeb thiab txhim khu kev qha cov khoom noj uas muaj cov khoom noj khoom haus; rau kev txhim kho thiab kev siv ntawm tsib-leaved chaste ntoo muab kev sim hauv paus; txhim kho qhov kev siv piv ntawm cov khoom siv cog, tsim kev lag luam siab.
Tsib-leaved chaste ntoo (Vitex negundo Linn) yog Verbenaceae Vitex hom, lwm lub npe tsib-leaved chaste ntoo bar, Fructus Viticis Negundo, cloth chaste tree, twigs ntawm tsob ntoo chaste, tsib ntiv tes cua, Folium vilicis Negundo. txhua xyoo machaka lossis dungarunga, thiab cog qhov siab tuaj yeem ncav cuag 6m, thiab ceg, nplooj thiab qia tag nrho muaj cov ntxhiab tsw, los ntawm cov ceg hauv paus, thiab kaw cov tawv nqaij zoo nkauj plaub hau.Nplooj yog mus rau lub neej, thiab palmately compound nplooj, muaj ntev kov, nplooj ntawv 3 -5 daim ntawv, thiab lub teeb ntsuab, yog ellipticity avette rau lanceolar, tag nrho ntawm ntug los yog me ntsis sawtooth, cov plaub hau dawb zoo ntawm lub neej nyob ze rau sab nraub qaum, rubbing muaj peat-reek.Qhov tsim nyog hav zoov ntawm tsib-leaved chaste ntoo nyob rau hauv lub torrid cheeb tsam thiab Temperate Region nyob rau hauv Tuam Tshoj, yog faib dav nyob rau hauv Tuam Tshoj Yangtze hav thiab txhua lub xeev thiab cheeb tsam, sab qab teb, thiab kuj muaj tis nyob rau hauv Shandong.Eastern Africa kuj dav faib thoob plaws hauv av xws li Bolivia ntawm Madagascar, sab qab teb sab hnub tuaj, Asia thiab South America.
Yellow vitex noob, nplooj, ceg thiab hauv paus tag nrho yuav siv tau los ua tshuaj.Yellow vitex noob muaj hnoos-relieving apophlegmatic thiab alleviates cov nyhuv ntawm bronchospasm, kho tsuas yog mob khaub thuas, hnoos, hawb pob, wandering mob caj dab, malaria, mob plab, hernia, qhov quav fistula. thiab lwm yam.Negundo Chastetree Nplooj tuaj yeem txo qhov superficies los ntawm kev ua kom txias, tshem tawm cov ntub dej, tshem tawm cov co toxins, kho feem ntau yog mob khaub thuas, heatstroke, ntuav thiab raws plab, kab mob plab, malaria, jaundice, rheumatism, kho o thiab mob los ntawm kev raug mob, thiab tuaj yeem tiv thaiv qhov mob. Kev loj hlob ntawm formaldehyde sacroiliitis o.Lub decoction ntawm Negundo Chastetree Nplooj los yog hauv paus muaj inhibiting nyhuv rau bacillus xws li streptococcus aureus, beta hemolytic streptococcus thiab cov hnyuv loj, anthrax, diphtheria, typhoid fever, ntsuab pus, dys.
Tsib-leaved chaste ntoo nroj tsuag tseem ceeb roj, kuj hais tias cov roj tsw qab los yog volatile roj, yog ib tug chav kawm ntawv cog-sourced theem nrab metabolism hauv chav kawm ntawv cov ntaub ntawv, yog molecular hnyav nyob rau hauv cov ntaub ntawv cog, muaj peev xwm steams nrog dej vapour, muaj lub volatility oily kua tshuaj ntawm tej yam tsw. .Qhov tseem ceeb roj feem ntau yog muab cov txiv hmab txiv ntoo, paj, nplooj thiab cov hauv paus hniav los ntawm cov nroj tsuag, muaj cov tshuaj tsw qab muaj zog los yog tsw ntxhiab.Cov tshuaj muaj pes tsawg leeg muaj qhov nyuaj, tuaj yeem muab faib ua aliphatics, aromatic series thiab terpene peb hom loj thiab lawv muaj. oxygen derivative li cawv, aldehyde, ketone, acid, ether, ester, lactone thiab lwm yam los ntawm cov qauv tshuaj, kuj muaj nyob rau hauv ntxiv nitrogenous thiab compound sulfur-bearing.Conventionally nroj tsuag tseem ceeb roj yog siv los npaj cov essence thiab flavoring tus neeg sawv cev, tab sis nyob rau hauv lub xeem. ob peb xyoos, cov tshuaj tiv thaiv kab mob ntawm cov nroj tsuag tseem ceeb roj thiab ib qho kev tivthaiv ntawm no tau ua tiav rau ntau qhov kev tshawb fawb hauv tsev thiab txawv teb chaws. Kev tshawb fawb qhia tau hais tias cov nroj tsuag tseem ceeb roj muaj cov tshuaj tua kab mob, desinsection, anti-oxidant isoreactivity, ntawm yam xws li tshuaj, tshuaj ua liaj ua teb, fodder additives, tau dav siv.
Tsib-leaved chaste ntoo volatile roj muaj qhov tseem ceeb ntawm kev siv tshuaj tua kab rau Main Stored Grain Kab xws li sitophilus zea-mais, Callosobruchus chinensis, tsawg dua nplej borers, thiab muaj peev xwm tswj tau zoo Fl rau kev tsim ntawm cov pejxeem, txo nws cov kom muaj nuj nqis.Monomerpen Terpane, fir Txhua tus muaj cov tshuaj tua kab ntau dua rau corundum Sitophilusspp. imago, yog insecticide active tshuaj tseem ceeb nyob rau hauv tsib-leaved chaste ntoo volatile roj.Lub chaw ua hauj lwm chav distillations xws li Yang Haixia extract volatile roj los ntawm tsib-leaved chaste ntoo.Siv roj chromatography/mass spectrometry technology (GC.MS) los kawm cov tshuaj muaj pes tsawg leeg ntawm tsib-leaved chaste ntoo volatile roj.Be sib cais mus rau tag nrho cov 37 tebchaw, txheeb xyuas qhov twg 28.Mainly muaj caryophyllene (23.981%).Huang Qiong (2008) thiab lwm yam. extract cov volatile roj ntawm Vitex negundo var cannabifolia nrog microwave irradiation. capillary gas chromatography ib qho MS ua ke nrog kev tshawb fawb hauv computer, nws cov tshuaj muaj pes tsawg leeg yog nqa tawm raws li kev tshuaj xyuas thiab kev txheeb xyuas, los ntawm thaj chaw normalization txoj kev, ntsuas cov ntsiab lus txheeb ze ntawm txhua qhov sib xyaw hauv cov roj tsis hloov pauv.Qhov txiaj ntsig txheeb xyuas 16 cov sib xyaw ua ke, thiab volatilization lub ntsiab lub cev ntawm roj yog caryophyllene (20.14%).
Extract ntau cov pa extracting txoj kev ntawm cov nroj tsuag volatile roj thiab muaj chav distillation (dej distillation txoj kev, distilling saum dej txoj kev, chav distillation), dej diffusion txheej txheem, hnyav extraction method, absorption method, supercritical CO2abstraction txheej txheem, ultrasonic yoj auxiliary extraction technology, microwave hluav taws xob induction abstraction txheej txheem, enzyme extraction technology etc.Shortcoming yog ua kom puas loj rau tshav kub-rhiab khoom thiab tsis ruaj khov constituents.
Cov ntsiab lus ntawm qhov invention
Lub hom phiaj ntawm qhov invention yog muab ib hom kev siv ib txhij distillation txoj kev, siv txoj kev npaj ntawm opposed polarity organic solvent extraction tsib-leaved chaste ntoo volatile roj.
Cov txheej txheem ntawm kev tsim tam sim no yog, nws yog tus cwj pwm nyob rau hauv qhov kev siv thiab hnyav 10g tsib-leaved chaste ntoo hmoov nyob rau hauv lub round-bottomed flask ntawm 1000mL, ntxiv 300mL distilled dej thiab ua kom ntau submergence khoom, cais tau 50mL ib txwm hexane nyob rau hauv 500mL flask. , txuas distilling thiab rho tawm cov cuab yeej ib txhij, ua cov khoom ib kawg kom txog 110 ± 5 ℃ ntawm qhov kub thiab txias me ntsis, cov organic hnyav-ib txwm hexane qhov kawg kub yog tswj ntawm 80 ℃ ± 5 ℃, kho tag nrho cov reflux hauv ob sab pib lub sijhawm thiab tuav 4h, tom qab rho tawm, cov organic reagent raug xa mus rau hauv cov cuab yeej ntsaws daim duab peb sab, ntxiv anhydrous sodium sulphate kom ua zoo-grannular tsis muaj loj caking, tub yees thaum hmo ntuj, tom qab hla lub millipore pom ntawm 0.45 μ m, rotary evaporation yog rau residual ntawm a Qhov me me, hloov pauv hauv cov qauv txhaj tshuaj lub raj mis thiab nitrogen tshuab kom tsis muaj ntxhiab tsw ntxhiab, tau cov roj tsis muaj zog, muaj zog peat-reek, cov roj tseem ceeb no yog nqa mus rau GC-MS hauv online tsom xam, organic reagent ib txwm hexane hloov. thiab ua rau hexanaphthene (90 ℃ ± 5 ℃ ntawm qhov kub), methylene dichloride (50 ℃ ± 5 ℃), ethyl acetate (90 ℃ ± 5 ℃) thiab siv tib txoj kev thiab nqa tawm thaum distillation extraction, distillation extraction yog cov qauv aqueous. cov tshuaj thiab cov organic reagent tau muab tso rau hauv feem rau ob sab ntawm cov cuab yeej thiab yog rhuab mus rau boiling ib txhij, dej vapor thiab hnyav vapo (u) r tag nrho sib tov nyob rau hauv ntaus ntawv, ib txhij condensation yog tawm thiab cov organic hnyav tivthaiv nyob rau hauv aqueous theem muab rho tawm tas li. tseem nyob rau hauv cov txheej txheem qias neeg raws li ntev, vim hais tias cov dej thiab cov organic theem tsis yaj ib leeg nyob rau hauv U-puab yeeb nkab thiab yuav tsum tau muab cais, yuav tsum rov qab mus rau feem nyob rau hauv lub hwj ntawm ob sab, los ntawm distillation, extraction txheej txheem nruam, ncig, ncav cuag. khoom ntawm cov volatile thiab semi-volatile compounds ntawm kab nyob rau hauv extraction, sib cais thiab enrichment qauv.
Raws li tau txais cov txheej txheem txheej txheem, cov txheej txheem ntawm kev tshuaj ntsuam xyuas tau muab rho tawm los ua haujlwm siab, yooj yim rau kev khiav lag luam; Siv rau kev khaws cia ntawm cov lotus rhizome tshiab, cov nyhuv zoo heev; Pab txhawb kom txhim kho cov ntsiab lus ntawm lub hom phiaj compound.

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    Nws invention muaj feem xyuam rau thaj tsam ntawm vitex negundo linn volatile roj, thiab tshwj xeeb tshaj yog muaj feem xyuam rau ib txoj kev npaj ntawm vitex negundo linn volatile roj. Txoj kev npaj yog tus cwj pwm los ntawm kev suav nrog cov kauj ruam hauv qab no: hnyav 10g ntawm vitex negundo linn hmoov hauv 1000mL puag ncig-hauv qab khob; ntxiv 300mL ntawm cov dej distilled kom tag nrho rau hauv cov khoom; ntxiv 50mL ntawm ib txwm hexane nyob rau hauv 500mL hwj; txuas ib txhij distillation-extraction ntaus ntawv, nyob rau hauv ib qho kawg ntawm cov khoom tuav ib tug micro-boiling xeev ntawm txog 110+/-5 DEG C; tom qab rho tawm, hloov cov organic reagent mus rau ib lub raj mis peb sab nrog lub ntsaws kom tau cov roj daj daj; Raws li cov theem aqueous thiab cov organic theem yog immiscible thiab yog sib cais nyob rau hauv ib tug U-shaped raj thiab feem ntws rov qab mus rau lub flasks ntawm ob sab, paub lub hom phiaj ntawm extracting, sib cais thiab enriching ib tug volatile thiab non-volatile Cheebtsam nyob rau hauv ib tug qauv los ntawm ib tug tas mus li thiab ncig distillation thiab extraction txheej txheem. Los ntawm kev siv cov txheej txheem thev naus laus zis, cov thev naus laus zis thev naus laus zis tau tshuaj xyuas muaj cov yam ntxwv ntawm kev rho tawm siab thiab yooj yim rau kev khiav lag luam. Txoj kev npaj yog siv los khaws cov paj tshiab nrog cov txiaj ntsig zoo. Txoj kev npaj yog qhov zoo rau kev txhim kho cov ntsiab lus ntawm lub hom phiaj teeb meem.








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